By D Pletcher, R Greff, R Peat, L.M. Peter, D. Pletcher
Utilizing 372 references and 211 illustrations, this ebook underlines the basics of electrochemistry necessary to the certainty of laboratory experiments. It treats not just the basic suggestions of electrode reactions, but additionally covers the method and functional program of the numerous flexible electrochemical thoughts available.
- Underlines the basics of electrochemistry necessary to the knowledge of laboratory experiments
- Treats the basic innovations of electrode reactions
- Covers the technique and functional software of the numerous flexible electrochemical ideas available
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Extra info for Instrumental Methods in Electrochemistry
Which scheme is followed depends on the relative rates of the various steps, and under certain circumstances the reaction follows both routes. The differentiation between disp 1 and ece reactions is most readily achieved by optical techniques, and this will be discussed in Chapter 10, but it is also possible by double potential step chronoamperometry [14). The application of pulse techniques to the determination of the kinetics of coupled homogeneous chemical reactions will now be discussed. Potential step techniques Sec.
Anson, J. Electroanal. Chem. 65 (1975) 711, 737, and 759. E. Gillet, Chem. Ing. Techn. 40 (1968) 573. (5] B. Kastening & G. Kazemifard, Ber Bunsenges. Phys. Chem. 74 (1970) 551. Relevant reading (1) W. J. Albery, Electrode processes, Clarendon Press, 1975. (2) J. O'M Bockris & A. K. N. Reddy, Modern electrochemistry - Volume 2, Plenum Press, 1970. (3) A. J. Bard & L. R. Faulkner, Electrochemical methods, John Wiley and Sons, 1980. 2 Steady state and potential step techniques As will now be clear from the first Chapter, electrochemical processes can be rather complex.
The application of these techniques is the subject of this and subsequent chapters. Throughout the emphasis will be placed on (a) developing diagnostic tests to be used in the elucidation of reaction mechanisms, [Sec. 1] Steady state techniques 43 (b) demonstrating how quantitative data for single reaction steps may be obtained. e. when current flows the electron transfer is insufficiently fast to maintain Nernstian equilibrium at the electrode surface. In such cases kinetic data can be obtained directly from steady state current-voltage measurements analysed on the basis of the Tafel equations (see Fig.